Habb-e-asgand, Habb-e-suranjan and Halwa Gheekwar are the Unani Formulations mainly used for various ailments like arthritis, gout, joint Pain, inflammations, anticancer, antioxidant, and immunomodulator. Unani Formulations are quite safe and effective. Although the formulations of the Unani system of medicine are more recognized, not so much scientific work has been reported so far. Many Pharmaceutical Companies manufacture the formulation for commercial supply but they fail to maintain the desired standards for it. The Unani Formulations was subjected to evaluate physiochemical parameters like Foreign Content, LOD, Ash Value, Extractive Value, Heavy Metals Estimation, Pesticide Residue, Test for Aflatoxins and were found to be under the limit and microbial content were also execute to check the presence of any hazardous substance in the formulation. The evidence produced in this study will lead to develop pharmacopeial standards of Habb-e-asgand, Habb-e-suranjan and Halwa Gheekwar which eventually assist to estimate the Standard, safety and potency of the formulation.